Open Access Experiment Lists

The tables below summarises the experiments available through the fully automated open-access NMR spectrometers situated close to the organic synthetic laboratories. This list may also be downloaded. A greater range of experiments are available for trained users through use of the bookable spectrometers.

 

n = normal (single) experiments

c = composite experiments composed of two or more parameter sets

 

 

Experiments available on the DPX200 spectrometer

Experiment
Description
Range (ppm)
Number of transients
Run time (min:sec)
Night time only
N h1acq.au
Proton
12 → -2
16
1:15
 
N h1acq2.au
Proton with wide SW
21 → -5
16
1:19
 
N h1acq3.au
Proton with extra wide SW to 25 ppm 
25 → -5
16
1:12
 
N h1sup.au
Proton with D2O presatutation
13 → -3
16
1:09
 
N h1sup2.au
Proton with wide SW and D2O presaturation
21 → -11
16
1:09
 

 

Experiments available on the AVG400 spectrometer

Experiment
Description
Range (ppm)
Number of transients
Run time (min:sec)
Night time only
N h1acq.crl
Proton
16 → -4
16
1:32
 
N h1sup.crl
Proton with D2O presaturation
14.7 → -5.3
16
1:32
 
N f19acq.crl
Fluorine 100 to -250 ppm (16 scans)
100 → -250
16
1:00
 
N f19dec.crl
Fluorine with 1H decoupling 100 to -250 ppm (16 scans)
100 → -250
16
1:00
 
N f19acqQ.crl
Fluorine quantitative -50 to -250 ppm (set o1p for 19F shift)
-50 → -250
16
3:38
 
N h1f19dec.crl
Proton with 19F decoupling (set o2p for 19F shift)
15 → -5
16
0:55
 
N p31dec.crl
Phosphorus with 1H decoupling 200 to -200 ppm
200 → -200
16
1:01
 
Nh1p31dec.crl
Proton with 31P decoupling (set o2p for 31P shift)
15 → -5
16
0:55
 
n c13acq_256.crl
13C 256 scans
230 → -30
256
7:20
Yes
n c13acq_512.crl
13C 512 scans
230 → -30
512
14:33
Yes
n DEPT135.crl
13C DEPT135
230 → -30
128
3:41
Yes
n DEPTQ.crl
13C DEPTQ
230 → -30
128
7:16
Yes
n f19acq_256.crl
Fluorine 100 to -250 ppm (256 scans)
100 → -250
256
13:07
Yes
n f19dec_256.crl
Fluorine with 1H decoupling 100 to -250 ppm (256 scans)
100 → -250
256
13:07
Yes
c COSYSW
Proton with 2D COSY
optimised on 1H 
1
5
Yes
c COSYPRSW
Proton presat. with 2D COSY 
optimised on 1H 
1
6
Yes
c HSQCSW
13C edited HSQC
optimised on 1H 
2
5
Yes

 

Experiments available on the AVH400  spectrometer

Experiment
Description
Range (ppm)
Number of transients
Run time (min:sec)
Night time only
N h1acq.crl
Proton
16 → -4
16
1:32
 
N h1acq2.crl
Proton with wide SW
25 → -5
16
1:07
 
N h1sup.crl
Proton with D2O presaturation
14.7 → -5.3
16
1:32
 
n f19acq.crl
Fluorine 100 to -250 ppm (16 scans)
100 → -250
16
1:00
Yes
n f19acq_256.crl
Fluorine 100 to -250 ppm (256 scans)
100 → -250
256
13:07
Yes
n f19dec.crl
Fluorine with 1H decoupling 100 to -250 ppm (16 scans)
100 → -250
16
1:00
Yes
n f19dec_256.crl
Fluorine with 1H decoupling 100 to -250 ppm (256 scans)
100 → -250
256
13:07
Yes
n h1f19dec.crl
Proton with 19F decoupling (set o2p for 19F shift)
15 → -5
16
0:55
Yes
n p31dec.crl
Phosphorus with 1H decoupling 200 to -200 ppm
200 → -200
16
1:01
Yes
n h1p31dec.crl
Proton with 31P decoupling (set o2p for 31P shift)
15 → -5
16
0:55
Yes
n c13acq_256.crl
Carbon 256 scans
230 → -30
256
7:20
Yes
n c13acq_512.crl
Carbon 512 scans
230 → -30
512
14:33
Yes
n DEPT135.crl
Carbon DEPT135
230 → -30
128
3:41
Yes
n DEPTQ.crl
Carbon DEPTQ
230 → -30
128
7:16
Yes
c COSY.comp
Proton with COSY
optimised on 1H 
1
5
Yes
c COSYPR.comp
Proton presat. with COSY 
optimised on 1H 
1
5
Yes
c HSQC.comp
Proton with HSQC
optimised on 1H 
2
5
Yes
c COSY_HSQC.comp
Proton with COSY and HSQC
optimised on 1H 
1 + 2
5 + 5
Yes

Experiments available on the AVF400 spectrometer 

Experiment
Description
Range (ppm)
Number of transients
Run time (min:sec)
Night time only
N h1acq.crl
Proton
16 → -4
16
1:32
 
N h1acq2.crl
Proton with wide SW
25 → -5
16
1:07
 
N h1sup.crl
Proton with D2O presaturation
14.7 → -5.3
16
1:32
 
n c13acq_256.crl
Carbon 256 scans
230 → -30
256
7:20
Yes
n DEPT135.crl
Carbon DEPT135
230 → -30
128
3:41
Yes
n DEPTQ.crl
Carbon DEPTQ
230 → -30
128
7:16
Yes
c COSY.comp
Proton with COSY
optimised on 1H 
1
5
Yes
c COSYPR.comp
Proton presat. with COSY 
optimised on 1H 
1
6
Yes
c HSQC.comp
Proton with HSQC
optimised on 1H 
2
5
Yes
c COSY_HSQC.comp
Proton with COSY and HSQC
optimised on 1H 
1 + 2
5 + 5
Yes
N f19acq.crl
Fluorine 100 to -250 ppm (16 scans)
100 → -250
16
1:00
 
N f19dec.crl
Fluorine with 1H decoupling 100 to -250 ppm (16 scans)
100 → -250
16
1:00
 
N f19acqQ.crl
Fluorine quantitative -50 to -250 ppm (set o1p for 19F shift)
-50 → -250
16
3:38
 
C F19.comp
Fluorine optimised for JH measurement 
optimised on 19F
16
0:38
 
N h1f19dec.crl
Proton with 19F decoupling (set o2p for 19F shift)
15 → -5
16
0:55
 
n f19acq_256.crl
Fluorine 100 to -250 ppm (256 scans)
100 → -250
256
13:07
Yes
n f19dec_256.crl
Fluorine with 1H decoupling 100 to -250 ppm (256 scans)
100 → -250
256
13:07
Yes
N p31dec.crl
Phosphorus with 1H decoupling 200 to -200 ppm
200 → -200
16
1:01
 
N h1p31dec.crl
Proton with 31P decoupling (set o2p for 31P shift)
15 → -5
16
0:55